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Beilstein J. Org. Chem. 2011, 7, 127–134, doi:10.3762/bjoc.7.18
Graphical Abstract
Scheme 1: Synthetic routes to isoxazoles 7a–7e.
Scheme 2: Synthetic routes to isoxazoles 7f–7h.
Scheme 3: Benzaldehyde photocycloaddition to 7a–7e.
Scheme 4: Photochemical ring contraction of isoxazoles 7f–7h.
Scheme 5: Photocycloaddition of aromatic aldehydes to di- and trimethyl isoxazoles 7d and 7e.
Scheme 6: Preparative photocycloadditions of 7e with aromatic aldehydes.
Figure 1: Structures of the photoproducts 9a–9c in the crystal.
Scheme 7: T-type photochromism of isoxazole–aldehyde pairs.
Scheme 8: Reductive cleavage of the trimethylisoxazole adduct 9a.